Man in a white lab coat and a glove working at a vacuum chamber beside a monitor showing a process diagram

Laboratory of Thin Films

A combined system for magnetron sputtering and thermal evaporation of thin films, equipped with three magnetrons (one of which is radio-frequency powered) and a thermal evaporator. It allows the deposition of both conductive and dielectric layers, as well as co-deposition from two sources simultaneously.

Description of Activities

  • Deposition of nano- and micro-scale thin films of metals, oxides, semiconductors and non-conductive materials by direct-current (DC) and radio-frequency (RF) single (stand-alone) sputtering and co-sputtering
  • Vacuum thermal evaporation from one or more sources
  • Cleaning of the substrates before the start of the process
  • Ability to deposit films on various types of rigid (metal, glass, silicon) and flexible (polymer) substrates
Large stainless-steel vacuum chamber on a blue frame labelled KENOSISTEC KES 500 TC, with a control cabinet

Equipment

Combined system for magnetron sputtering and vacuum thermal deposition of layers, model KES 500 TC

The process chamber of the system has three magnetron cathodes, 5 cm in diameter, in confocal geometry with a “sputter up” configuration. The cathodes are water-cooled, and each is fitted with a special pneumatic protective shutter for pre-sputtering processes and a special shield to avoid possible cross-contamination. The system is equipped with a DC power supply, which can be connected to two of the cathodes via a system of 2 DC switches, and one 13.56 MHz radio-frequency power supply connected directly to the third cathode. This configuration allows the deposition of both conductive and dielectric layers (such as CeO2, SiO2, Al2O3, etc.). The target-to-substrate distance can be adjusted from inside the chamber. The vacuum attainable in the process chamber is better than 5 x 10-7 mbar.

The sample holder/anode in the process chamber can be loaded with samples 5 cm in diameter or with a square sample measuring 5 cm x 5 cm, and can rotate about its orthogonal axis so as to optimise the uniformity of the deposition as far as possible. At the same time, the anode can be heated to 300°C by a substrate heating system. The system has a second radio-frequency power supply connected to the sample holder.

Vacuum thermal evaporation is performed by a thermal evaporator mounted in the lower part of the chamber, with electrically powered thermal evaporation sources with a maximum current of 600 A.

Man in a white lab coat and a glove working at a vacuum chamber beside a monitor showing a process diagram

Gallery

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Access to the Laboratory of Thin Films

The Laboratory of Thin Films is part of the research infrastructure of the National Centre of Excellence “Mechatronics and Clean Technologies” and is located at the Geo Milev campus. Requests for access and for joint research are therefore handled centrally — see Contact. In addition, a full overview of the Centre’s other laboratories is available on the Infrastructure and Laboratories page.

The thin-film equipment was established under project BG16RFPR002-1.014-0006, funded by the “Research, Innovation and Digitalisation for Smart Transformation” Programme 2021–2027, co-funded by the European Union through the European Regional Development Fund.